FIELD: chemistry.
SUBSTANCE: method of phosphate ore processing includes one-step counterflow process of phosphate ore decomposition, characterised by P2O5 content exceeding 20% in weight, by processing it with water solution of hydrochloric acid, which has HCl concentration lower than 10% in weight, with formation of processing solution, consisting of water phase, in which calcium phosphate is in dissolved state, and of solid phase, which contains admixtures; preliminary neutralisation of processing solution, containing calcium phosphate in solution, to first pH value, which is lower than pH value, at which essential part of said dissolved calcium phosphate precipitates in form of calcium monohydrophosphate (DCP), with precipitation of admixtures; first separation of insoluble solid phase and water phase of processing solution; repeated neutralisation of water phase obtained during first separation to second pH value, exceeding said first pH value, with DCP precipitation; and second separation of repeatedly neutralised water medium, which represents water solution of calcium chloride and precipitated DCP.
EFFECT: method allows optimising ratio between dissolved P2O5 output and purity degree of final product and ensure economically profitable process, which can be realised on simple equipment.
14 cl, 3 dwg, 2 tbl, 1 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCTION OF PHOSPHORIC ACID | 2003 |
|
RU2300496C2 |
SOLID PHOSPHATE SALT AND METHOD OF ITS PRODUCTION | 2016 |
|
RU2627403C1 |
PHOSPHORUS-POTASSUIM-NITROGEN-CONTAINING NPK-FERTILISER AND METHOD FOR PRODUCING GRANULATED PHOSPHORUS-POTASSUIM-NITROGEN-CONTAINING NPK-FERTILISER | 2016 |
|
RU2626947C1 |
PHOSPHOR-POTASSIUM-NITROGEN-CONTAINING NPK-FERTILISER AND METHOD OF PRODUCING GRANULATED PHOSPHOR-POTASSIUM-NITROGEN-CONTAINING NPK-FERTILISERS | 2016 |
|
RU2628292C1 |
METHOD FOR PRODUCING IRON PHOSPHATE FROM IRON-CONTAINING WASTE | 2022 |
|
RU2801188C1 |
METHOD FOR OBTAINING COMPLEX MINERAL FERTILISERS FROM PHOSPHATE ORE AND PLANT FOR ITS IMPLEMENTATION | 2016 |
|
RU2634936C2 |
METHOD OF PREPARING COMPLEX FERTILIZERS | 1999 |
|
RU2162071C2 |
METHOD OF PRODUCTION OF PURIFIED PHOSPHORIC ACID | 2006 |
|
RU2315709C1 |
PHOSPHOGYPSUM INTEGRATED PROCESSING METHOD | 2004 |
|
RU2258036C1 |
METHOD FOR PRODUCTION OF COMPLEX FERTILIZERS | 2005 |
|
RU2286320C1 |
Authors
Dates
2009-04-27—Published
2004-12-23—Filed