METHOD OF OBTAINING OXYCOBALAMINE Russian patent published in 2009 - IPC C07H23/00 

Abstract RU 2368618 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of obtaining oxycobalamine - catalyst for catalytic therapy of malignant growths through electrochemical reduction of Co3+ to Co2+ in cyanocobalamine in a membrane cell on a titanium cathode in galvanostatic mode at current density 5.0-15.0 A/dm2 in an aqueous solution of hydrochloric acid and temperature 28-40°C, with subsequent oxidation of the latter with atmospheric oxygen with formation of oxycobalamine and separation of the end product through precipitation from a water-acetone mixture while cooling.

EFFECT: increased output of desired product up to 80,0-90,0%.

4 ex, 2 tbl

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RU 2 368 618 C1

Authors

Vorozhtsov Georgij Nikolaevich

Dmitrieva Ninel' Dmitrievna

Kalija Oleg Leonidovich

Konarev Aleksandr Andreevich

Luk'Janets Evgenij Antonovich

Pankratov Andrej Aleksandrovich

Chissov Valerij Ivanovich

Solov'Eva Ljudmila Ivanovna

Jakubovskaja Raisa Ivanovna

Jakunina Tat'Jana Vasil'Evna

Dates

2009-09-27Published

2008-08-14Filed