FIELD: chemistry.
SUBSTANCE: invention relates to production of phosphorus salts, particularly sodium tripolyphosphate, which is used in food, household and chemical industries. The method of producing sodium tripolyphosphate involves neutralisation of wet-process phosphoric acid with calcined soda to molar ratio Na2O : P2O5 = 1.63 - 1.70 and subsequent thermal treatment of sodium phosphates. In this process neutralisation takes place in a single step, while keeping temperature of the process, time and concentration of acid within limits necessary for obtaining concentration of disodium phosphate of not more than 36% in a neutral solution.
EFFECT: temperature of the process is varied from 70 to 90°C, duration of the process from 90 to 120 minutes and concentration of acid from 35 to 50% H3PO4.
2 cl, 1 tbl, 1 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING SODIUM TRIPOLYPHOSPHATE | 2007 |
|
RU2361811C1 |
METHOD OF PRODUCING TRISODIUM PHOSPHATE | 2008 |
|
RU2372282C1 |
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RU2285663C1 |
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RU2375300C2 |
SODIUM TRIPOLYPHOSPHATE PRODUCTION PROCESS | 1998 |
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RU2148010C1 |
PROCESS FOR PREPARATION MONOBASIC SODIUM PHOSPHATE SOLUTION | 1991 |
|
RU2008256C1 |
SODIUM TRIPOLYPHOSPHATE PRODUCTION PROCESS | 2001 |
|
RU2200703C1 |
METHOD OF PREPARING SODIUM TRIPOLYPHOSPHATE | 1995 |
|
RU2159212C2 |
METHOD OF PRODUCTION OF THE ALKALI METALS PHOSPHATES | 2007 |
|
RU2318724C1 |
METHOD OF PRODUCING SODIUM TRIPOLYPHOSPHATE | 0 |
|
SU874617A1 |
Authors
Dates
2010-01-10—Published
2008-06-04—Filed