METHOD FOR SYNTHESIS OF DICHLORANHYDRIDE OF 2-(2,3-DICHLOROPROPOXY)ETHENYL PHOSPHONIC ACID Russian patent published in 2010 - IPC C07F9/42 

Abstract RU 2387662 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method for synthesis of dichloranhydride of 2-(2,3-dichloropropoxy)ethenyl phosphonic acid of formula (1), which can be used in organic synthesis: ClCH2CHClCH2OCH=CHP(O)Cl2, 1. The proposed method involves reaction of vinyl glycidyl ether with phosphorus pentachloride in molar ratio 1:2 in a medium of an inert organic solvent at temperature 0-20°C and subsequent treatment of the formed adduct with acetone.

EFFECT: design of a method for synthesis of an organic synthesis intermediate product.

1 cl, 2 ex

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RU 2 387 662 C1

Authors

Mitrasov Jurij Nikitich

Smolina Irina Nikolaevna

Kondrat'Eva Oksana Viktorovna

Frolova Marija Aleksandrovna

Dates

2010-04-27Published

2008-12-15Filed