METHOD FOR PRODUCING 2,3-DIHYDROFURIL-4-PHOSPHIC ACID DICHLOROANHYDRIDE Russian patent published in 2023 - IPC C07F9/42 

Abstract RU 2802467 C1

FIELD: chemistry.

SUBSTANCE: improved method for producing 2,3-dihydrofuryl-4-phosphonic acid dichloride of formula (1). A method is disclosed for producing 2,3-dihydrofuryl-4-phosphonic acid dichloride of formula (1) by reacting tetrahydrofuran with phosphorus pentachloride in an inert organic solvent at room temperature, followed by decomposition of the resulting adduct with an oxygen-comprising compound, characterized in that, in order to simplify the process, as an oxygen-comprising compounds, sodium percarbonate is used and the process is carried out at room temperature.

EFFECT: invention provides a significant simplification, increase in the yield and safety of the technological process, as well as the purity of the target product and a decrease in the amount of acid production waste due to their binding with sodium carbonate.

1 cl, 1 ex

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RU 2 802 467 C1

Authors

Mitrasov Yurij Nikitich

Savinova Nadezhda Petrovna

Gladkova Anastasiya Ivanovna

Dates

2023-08-29Published

2022-10-04Filed