METHOD OF PRODUCING 2-PHENYL-1,1,2-TRICHLOROETHYLPHOSPHONIC ACID DICHLORIDE Russian patent published in 2024 - IPC C07F9/42 

Abstract RU 2814257 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing 2-phenyl-1,1,2-trichloroethyl-phosphonic acid dichloride of formula C6H5CHClCCl2P(O)Cl2 by treatment of an adduct of styrene and phosphorus pentachloride with a sulfuric acid derivative in a medium of an inert organic solvent, in order to simplify the process, the sulfuric acid derivative used is hydroxylamine sulphate and the process is carried out at room temperature.

EFFECT: development of a new method of producing 2-phenyl-1,1,2-trichloroethylphosphonic acid of formula C6H5CHClCCl2P(O)Cl2, characterized by reaction at room temperature, and also does not require use of toxic reagents.

1 cl, 2 ex

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RU 2 814 257 C1

Authors

Mitrasov Iurii Nikitich

Savinova Nadezhda Petrovna

Afanaseva Kristina Sergeevna

Lukicheva Nadezhda Aleksandrovna

Dates

2024-02-28Published

2023-08-11Filed