METHOD OF PRODUCING PALLADIUM PROPIONATE Russian patent published in 2011 - IPC C07F15/00 

Abstract RU 2430926 C1

FIELD: chemistry.

SUBSTANCE: method involves dissolving palladium metal in concentrated nitric acid and evaporating the obtained solution. Before crystallisation of palladium (II) nitrate at solution temperature (20-80)°C, an anhydride of propionic acid is proportionally added to the palladium nitrate solution after evaporation in amount of (1.5-3.0) l anhydride of propionic acid per 1 kg of the initial palladium metal for (10-30) minutes. The formed solution is heated to (90-110)°C for (30-60) minutes and the obtained solution or suspension is cooled to temperature not higher than 20°C, with duration of crystallisation of the product not less than 6 hours.

EFFECT: invention provides a stable method of producing palladium propionate in crystalline mono-phase state [Pd3(C2H5COO)6] and simplifies the production method.

1 ex, 1 tbl

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RU 2 430 926 C1

Authors

Mulagaleev Ruslan Faatovich

Kirik Sergej Dmitrievich

Dates

2011-10-10Published

2010-01-20Filed