FIELD: chemistry.
SUBSTANCE: invention relates to an improved method of drying aromatic carboxylic acid, involving drying of aromatic carboxylic acid precipitate using a fluidised bed drier, where the precipitate is fed into the drier at a rate of 50 kg/h or higher, and a drying gas at temperature 80-160°C is fed into the drier with reduced speed of 0.3-1 m/s, so that content of liquid in the precipitate is equal to or less than 14 wt %; as well as to an improved method of obtaining dry aromatic carboxylic acid, involving continuous drying of aromatic carboxylic acid precipitate using a fluidised bed drier to obtain ready aromatic carboxylic acid, where the precipitate is fed into the drier at a rate of 50 kg/h or higher, and drying gas at temperature 80-160°C is fed into the drier at reduced speed of 0.3-1 m/s so that content of liquid in the precipitate is equal to or less than 14 wt %. The aim of the invention is to develop a method of drying aromatic carboxylic acid and a method of drying aromatic carboxylic acid, each method solving problems associated with use of a fluidised bed drier, such as clogging by crystals or aromatic carboxylic acid crystals sticking in the drier, and low efficiency of the drier.
EFFECT: ensuring stable operation of a fluidised bed drier.
8 cl, 5 dwg, 1 tbl, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING AROMATIC CARBOXYLIC ACID | 2008 |
|
RU2467998C2 |
RECOVERY OF AROMATIC CARBOXYLIC ACIDS AND OXIDATION CATALYST | 2011 |
|
RU2575125C2 |
METHOD OF PREPARING AROMATIC CARBOXYLIC ACIDS AND METHOD OF PREPARING PURIFIED NAPHTHALENEDICARBOXYLIC ACID | 1993 |
|
RU2128641C1 |
METHOD OF PREPARING DRY RESIDUE OF CARBOXYLIC ACID SUITABLE FOR SYNTHESIS OF POLYESTERS | 2005 |
|
RU2380352C2 |
METHOD AND APPARATUS FOR PRODUCING AROMATIC CARBOXYLIC ACIDS (VERSIONS) | 2006 |
|
RU2449980C2 |
PRODUCTION OF AROMATIC CARBOXYLIC ACIDS | 2011 |
|
RU2574394C2 |
METHOD AND APPARATUS FOR PRODUCING AROMATIC CARBOXYLIC ACIDS | 2006 |
|
RU2414448C2 |
METHOD OF RECOVERING ENERGY DURING PRODUCTION OF AROMATIC CARBOXYLIC ACIDS | 2006 |
|
RU2435754C2 |
IMPROVED METHOD AND DEVICE FOR PRODUCTION OF AROMATIC CARBOXYLIC ACIDS | 2014 |
|
RU2687489C1 |
METHOD OF PURIFICATION OF RAW CARBOXYLIC ACID SUSPENSION | 2003 |
|
RU2341512C2 |
Authors
Dates
2012-03-10—Published
2007-06-07—Filed