FIELD: chemistry.
SUBSTANCE: invention relates to a novel method for synthesis of N,N-dimethylacetamide, which is widely used as a solvent in different fields, involving reaction of ethyl acetate (EA) and N,N-dimethylamine (DMA) in the presence of polyethylene polyamines (PEPA), having formula NH2[(CH2CH2)NH]n-1CH2CH2NH2, where n = 2-4, as a catalyst, where separate compounds of this group or their mixtures can be used.
EFFECT: high output of the end product (dimethylacetamide) of high quality (more than 99,9% content of basic substance) due to a simpler step for separating the catalyst from the reaction products.
3 cl, 16 ex, 1 tbl
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Authors
Dates
2012-05-10—Published
2010-03-31—Filed