1,5-BIS[(TERT-BUTYLAMINO)METHYL]-N,N'-DI-TERT-BUTYLBISPIDIN-9-ONE AND METHOD FOR PRODUCTION THEREOF Russian patent published in 2013 - IPC C07D471/08 C07D471/20 

Abstract RU 2472793 C1

FIELD: chemistry.

SUBSTANCE: invention relates to organic chemistry and specifically to 1,5-bis[(tert-butylamino)methyl]-N,N'-di-tert-butylbispidin-9-one and a method for production thereof. 1,5-bis[(tert-butylamino)methyl]-N,N'-di-tert-butylbispidin-9-one is obtained by condensation of acetone with 1,3,5-tri-(tert-butyl)-1,3,5-triazacyclohexane while heating in an alcohol in the presence of acetic acid. The reaction is carried out while heating in ethanol or another alcohol. The obtained product is extracted after condensation of the reaction mass in a vacuum with hot toluene and recrystallised from ethyl alcohol.

EFFECT: obtaining a novel compound which can be used as a starting substance when producing bispidine and 1,3-diazaadamantane derivatives.

2 cl, 3 ex

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RU 2 472 793 C1

Authors

Kuznetsov Anatolij Ivanovich

Senan Ibragim Mokhammed Khasan

Dates

2013-01-20Published

2011-07-20Filed