FIELD: chemistry.
SUBSTANCE: method of producing alkyd resin involves feeding and mixing in a reactor an oil-containing component, glycerine and LiOH, and heating the mixture to 230-260°C, followed by vinylation, polyesterification and bringing to the required characteristics by adding a solvent, wherein vinylation is preceded by alcoholysis, distillation of water without an azeotrope and an alcohol test; after the alcohol test the mixture is cooled to 150-160°C and then undergoes vinylation in the presence of vinyl toluene, xylene, phthalic anhydride and di-tertiary butyl peroxide.
EFFECT: high efficiency of the process and low power consumption owing to a shorter time for synthesis of the alkyd mixture; the obtained resin has improved colour characteristics and shorter drying time to 3rd degree.
7 cl, 1 tbl
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Authors
Dates
2013-04-27—Published
2011-10-20—Filed