METHOD OF PRODUCING FULLERENE-POLYSULPHONIC ACID Russian patent published in 2013 - IPC C01B31/02 B82B3/00 B82Y40/00 

Abstract RU 2484012 C1

FIELD: chemistry.

SUBSTANCE: invention relates to chemical industry and medicine and can be used in producing concrete plasticisers, microbiocides with anti-HIV properties which are not cytotoxic and modifiers of epoxy composites. Fullerene-polysulphonic acid is a water- and alcohol-soluble product of reaction of coal tar and coal tar pitch with sulphuric acid with concentration of at least 80%. Unreacted sulphuric acid formed when treating sulphonic acid and unreacted aromatic hydrocarbons are successively washed off with toluene, carbon tetrachloride and acetone to pH 6.5-7.0. Fullerene-polysulphonic acid is then extracted with ethyl alcohol in Soxhlet apparatus. Ethyl alcohol is distilled from the alcohol solution of fullerene-polysulphonic acid to dry residue.

EFFECT: invention enables to obtain fullerene-polysulphonic acid using a simple method using cheap and readily available reactants.

7 cl, 2 dwg, 2 ex

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RU 2 484 012 C1

Authors

Kozeev Evgenij Aleksandrovich

Kozeev Aleksandr Alekseevich

Ivanova Ljudmila Vladimirovna

Dates

2013-06-10Published

2011-11-22Filed