FIELD: chemistry.
SUBSTANCE: invention can be used in chemical industry. The method of producing sodium chloride comprises the following steps: (i) preparing a salt solution with sodium chloride concentration higher than that of sodium chloride at the eutectic point, but lower than in a saturated salt solution, by dissolving a sodium chloride source in water; (ii) cooling the obtained salt solution using an intermediate coolant in a self-cleaning heat-exchanger with a fluidised bed or in a crystalliser to temperature below 0°C, but higher than the eutectic point of the obtained salt solution, to obtain a suspension containing a sodium chloride dihydrate and a mother solution; (iii) feeding the sodium chloride dihydrate into a recrystallisation apparatus to form sodium chloride and a mother solution, and (iv) recycling at least a portion of the mother solution obtained at step (ii) and/or step (iii) to step (i).
EFFECT: invention reduces power consumption of industrial production of sodium chloride from underground deposits, increases purity of the obtained sodium chloride without conducting purification step and evaporative crystallisation steps.
9 cl, 1 dwg, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING SODIUM CHLORIDE | 2009 |
|
RU2494044C2 |
METHOD AND REACTOR FOR EXTRACTING SODIUM CHLORIDE AND POTASSIUM CHLORIDE FROM POLYMINERAL SOURCES | 2018 |
|
RU2669622C1 |
METHOD OF PREPARING POTASSIUM SULFATE, SODIUM SULFATE AND SODIUM CHLORIDE | 1995 |
|
RU2157791C2 |
METHOD OF CONTINUOUSLY PRODUCING POTASSIUM SULFATE FROM SODIUM SULFATE | 1994 |
|
RU2107028C1 |
METHOD OF PRODUCTION OF POTASSIUM SULFATE AND SODIUM SULFATE (VERSIONS) | 1995 |
|
RU2176218C2 |
METHOD FOR PRODUCTION OF POTASSIUM SULFATE | 1994 |
|
RU2105717C1 |
METHOD FOR TREATING WASTES RESULTING FROM PROCESSING CRUDE POTASSIUM SALTS AND CONSTITUTED, PREDOMINANTLY, BY SODIUM SULFATES | 1994 |
|
RU2108972C1 |
METHOD FOR CONTINUOUS SYNTHESIS OF 4-NITROSOPHENOL | 2021 |
|
RU2762969C1 |
METHOD FOR PRODUCING POTASSIUM SULFATE FROM POTASH AND SODIUM SULFATE | 1999 |
|
RU2235065C2 |
METHOD OF EXTRACTION OF SODIUM SULFATE AND CHLORIDE FROM MINERALIZED WATER | 2004 |
|
RU2281258C2 |
Authors
Dates
2014-01-20—Published
2009-10-29—Filed