FIELD: chemistry.
SUBSTANCE: chromium phosphate is obtained in a reactor by dissolving chromium trioxide in water. Orthophosphoric acid and a stabilising additive - ethanol - are then added. A strong reducing agent - aqueous hydrazine-hydrate solution - is slowly added to the obtained mixture of chromic acid, orthophosphoric acid and ethanol in an amount which enables formation and maturation of chromium phosphate particles, suspension pH of 4-7 and concentration of chromium phosphate of 50-100 g/cm. The end product is then filtered and dried. The filtrate is returned to preparation of the mixture of chromium trioxide, orthophosphoric acid and ethanol.
EFFECT: invention simplifies the technique and completely prevents formation of waste water.
1 tbl, 6 ex
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Authors
Dates
2014-03-27—Published
2012-06-04—Filed