METHOD OF PRODUCING 5,7-BIS-(PHENYLAMINO)-4,6-DINITROBENZOFUROXANE Russian patent published in 2014 - IPC C07D271/12 

Abstract RU 2528828 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing 5,7-bis-(phenylamino)-4,6-dinitrobenzofuroxane, at temperature of 50-55°C by reacting 5,7-dichloro-4,6-dinitrobenzofuroxane with phenylamine. The process is carried out in water with potassium carbonate and ammonium chloride dissolved therein and in the presence of oxyethylated nonylphenol in molar ratio of 1:0.5:0.13, respectively. Molar ratio of 5,7-dichloro-4,6-dinitrobenzofuroxane to phenyl is equal to 1:2, respectively. Water is taken in amount of 1 g per 100 ml 5,7-dichloro-4,6-dinitrobenzofuroxane.

EFFECT: novel method which reduces consumption of phenylamine by half and increases output of the product.

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RU 2 528 828 C1

Authors

Jusupova Luiza Magdanurovna

Morogova Darina Evgen'Evna

Spatlova Lidija Valentinovna

Vasjutina Ekaterina Anatol'Evna

Dates

2014-09-20Published

2013-04-30Filed