FIELD: chemistry.
SUBSTANCE: method is carried out by treating nitromethyl-ONN-azoxy compounds of general formula (II) with a nitrating agent. The nitrating agent used is a mixture of concentrated nitric acid (HNO3) and dinitrogen tetroxide (N2O4). In formulae
and Z is an alkyl or N,O-containing heterocyclic radical.
EFFECT: method increases output of end products and cuts the duration of the reaction.
2 cl, 6 ex
Title | Year | Author | Number |
---|---|---|---|
3,3'-BIS(FLUORODINITROMETHYL-ONN-AZOXYFURAZANYL)FUROXANE AND METHOD OF OBTAINING THEREOF | 2014 |
|
RU2557552C1 |
BIS(FLUORODINYTHROMETHYL-ONN-AZOXY)AZOXYFURAZAN AND PREPARATION METHOD THEREOF | 2015 |
|
RU2581050C1 |
3,3'-BIS(FLUORODINITROMETHYL-ONN-AZOXY)-4,4'-DIFURAZANYL ETHER AND METHOD FOR PRODUCTION THEREOF | 2013 |
|
RU2536041C1 |
3-(TRINITROMETHYL-ONN-AZOXY)-4-NITRAMINOFURAZANS AND METHODS FOR PRODUCTION THEREOF | 2012 |
|
RU2485108C1 |
ONIUM SALTS OF 4- (1,1-DINITROETHYL 1-ONN-AZOXY) -3- (1H-TETRAZOL-5-YL) FUROXAN AND METHODS FOR THEIR PREPARATION | 2016 |
|
RU2615630C1 |
N,N'-METHYLENE-BIS(POLYNITRO-2,4,6,8,10,12-HEXAAZAISOWURTZITANE) AND METHODS FOR THEIR PREPARATION | 2022 |
|
RU2786221C1 |
NITRAMIN DERIVATIVES OF 2,6,8,10,12-PENTANITRO-2,6,8,10,12-HEXAAZAISOWURTZITANE AND METHODS FOR THEIR PREPARATION | 2021 |
|
RU2772602C1 |
SUBSTITUTED [(3-NITRO-1H-1,2,4-TRIAZOL-1-YL)-NNO-AZOXY]FURAZANES AND PRODUCTION METHOD THEREOF | 2020 |
|
RU2747110C1 |
SUBSTITUTED [(3,4-DINITRO-1H-PYRAZOLE-1-YL)-NNO-AZOXY]FURAZANS AND METHOD FOR SYNTHESIS THEREOF | 2020 |
|
RU2756321C1 |
METHOD FOR PRODUCING [1,2,3,4]-TETRAZINO-[5,6-e]-[1,2,3,4]-TETRAZINO-1,3,6,8-TETRAOXIDE | 2015 |
|
RU2593993C1 |
Authors
Dates
2015-07-27—Published
2014-06-06—Filed