METHOD OF PRODUCING CELLULOSE Russian patent published in 2016 - IPC D21C1/00 

Abstract RU 2574958 C1

FIELD: chemistry.

SUBSTANCE: method comprises the saturation and hydrolysis of raw material in a medium of a hydrolysis solution, filtering cellulose, washing with water, filtering and drying, accompanied by using cycles, which include heating the material to 115°C or lower, high-speed pulsed vacuum action with pressure change in the range of up to 5 mmHg in less than 10 s, and then holding under a vacuum and releasing the vacuum. The disclosed method is universal. As the hydrolysis solution a nitric or sulphur acid solution, or mixtures thereof, and an alkaline solution can be used. A spent acid solution from nitrocellulose production can be used, which is less costly.

EFFECT: obtaining cellulose of a required type from any cellulose-containing material, cutting the duration of the cellulose hydrolysis process by an order, reducing the process temperature while obtaining the required chemical and structural homogeneity of cellulose without using equipment of the Federal Environmental Industrial and Nuclear Supervision Service.

10 cl

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RU 2 574 958 C1

Authors

Veselov Vladimir Mikhajlovich

Abramov Jakov Kuz'Mich

Zalevskij Viktor Mikhajlovich

Tamurka Vitalij Grigor'Evich

Volodin Veniamin Sergeevich

Evdokimov Vladimir Dmitrievich

Mironov Boris Ivanovich

Vatueva Ol'Ga Borisovna

Gukasov Nikolaj Aleksandrovich

Marshannikova Ljudmila Mikhajlovna

Mordvinova Tat'Jana Mikhajlovna

Salomatina Natal'Ja Aleksandrovna

Sarychev Dmitrij Konstantinovich

Pil'Gun Aleksandr Ivanovich

Birjukova Valentina Ivanovna

Dates

2016-02-10Published

2014-11-05Filed