FIELD: chemistry.
SUBSTANCE: invention relates to a method, that enables to obtain reactivated alkane dehydrogenation catalyst. Treatment within a regenerator comprises following sequential steps: (a) heating deactivated catalyst to a temperature of at least 660 °C using heat generated by combusting coke, contained on partially deactivated catalyst, and a fuel source other than said coke; and (b) subjecting further deactivated catalyst at a temperature of at least 660 °C while exposing to a flow of an oxygen-containing gas, which essentially does not contain combustible hydrocarbons, carbon oxides and water vapour, for a period of time longer than two minutes. Method may also (optionally) include a step (c) for maintaining oxygen-containing reactivated catalyst from step (b) at a temperature of at least 660 °C while exposing reactivated catalyst to a flow of stripping gas that is substantially free of molecular oxygen and combustible materials.
EFFECT: present invention provides improved characteristics of catalyst and increased number of response/reactivation cycles.
7 cl, 13 tbl, 7 ex
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Authors
Dates
2017-01-23—Published
2012-07-11—Filed