METHOD OF OBTAINING COMPLEXES OF LANTHANOIDS WITH 5, 15-DIPHENYLTETRABENZOPORINIC Russian patent published in 2017 - IPC C07F5/00 C07D487/22 

Abstract RU 2622292 C1

FIELD: chemistry.

SUBSTANCE: method involves the reaction of phthalimide with zinc acetate at a temperature of 230-240°C for 20-30 min, fusion of the resulting 3-[(1-oxo-1H-isoindol-3-yl)methylene]-2,3-dihydro-1H-isoindole-1-one with phenylacetic acid and a lanthanide salt at a temperature 320-330°C for 50-60 min, isolation and purification of the desired products by chromatography.

EFFECT: higher yields of target compounds with fewer chemical stages.

2 cl, 9 dwg, 7 tbl, 7 ex

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RU 2 622 292 C1

Authors

Rasputin Anatolij Aleksandrovich

Koptyaev Andrej Igorevich

Galanin Nikolaj Evgenevich

Shaposhnikov Gennadij Pavlovich

Dates

2017-06-14Published

2016-06-21Filed