FIELD: chemistry.
SUBSTANCE: invention relates to 2-[4'-(2",6"-dimethylphenoxy)benzoyl]benzoic acid pseudochloride of the formula I , which can be used as a monomer in the synthesis of polyarylene phthalides, as well as to a process for the preparation of Compound I, Comprising reacting 2-(4'-fluorobenzoyl) benzoic acid with 2,6-dimethylphenol in the presence of K2CO3 on heating in N, N-dimethylacetamide and subsequent treatment of the resulting 2-[4'-(2",6"-dimethylphenoxy)benzoyl] benzoic acid with thionyl chloride.
EFFECT: obtaining a new phthalide monomer from which one can obtain aromatic polymers, in particular polyarylenephthalides, and wherein the polycondensation reaction is not complicated processes branching and crosslinking.
3 cl, 2 ex
Title | Year | Author | Number |
---|---|---|---|
2-[4'-(2",6"-DIMETHYLPHENOXY)BENZOYL]BENZOIC ACID AND THE METHOD OF PREPARATION OF THE INVENTION | 2016 |
|
RU2621343C1 |
THERMAL-RESISTANT POLYARYLENHFLALIDE AND METHOD OF ITS PRODUCTION | 2016 |
|
RU2625158C1 |
POLYARYLENE DIPHTHALIDES AND METHOD OF THEIR PREPARING | 2016 |
|
RU2631502C2 |
POLYMERIC ANIZOTROPIC CONDUCTING COMPOSITION GLUING MATERIAL AND GLUING METHOD | 2006 |
|
RU2322469C2 |
DERIVATIVES OF PHTHALIMIDINES AS INTERMEDIATE COMPOUNDS FOR SYNTHESIS OF MONOMERS USED IN MAKING HEAT-RESISTANT POLYMERS | 0 |
|
SU1012575A1 |
DERIVATIVES OF PHTHALIMIDINES AS MONOMERS FOR SYNTHESIS OF THERMOSTABLE POLYMERS | 0 |
|
SU1015610A1 |
0 |
|
SU349185A1 | |
0 |
|
SU452215A1 | |
4-AND/OR(5)-TERT-AMYL-2-BENZOYLBENZOLOIC ACID OR THEIR MIXTURE AS INTERMMEDIATE PRODUCT FOR SYNTHESIS OF 2-TERT-AMYLANTHRAQUINONE | 0 |
|
SU892858A1 |
Authors
Dates
2017-07-12—Published
2016-07-11—Filed