METHOD FOR PREPARING BITULIN DICINAMATE Russian patent published in 2018 - IPC C07J63/00 C07J75/00 

Abstract RU 2665578 C1

FIELD: technological processes.

SUBSTANCE: invention relates to a method for preparing betulin dincinnamate by acylation of betulin in which cinnamic acid is used as an acylating agent, wherein acylation is carried out by fusing betulin with cinnamic acid at a temperature of 220–230 °C for 5–7 minutes with a molar ratio of betulin to cinnamic acid equal to 1:4, followed by recrystallization of the desired product from ethanol. .

EFFECT: new method for preparing betulin dicynnamate is proposed, which shortens the duration of the process and eliminates the use of expensive and toxic reagents.

1 cl, 1 ex

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RU 2 665 578 C1

Authors

Levdanskij Aleksandr Vladimirovich

Levdanskij Vladimir Aleksandrovich

Kuznetsov Boris Nikolaevich

Dates

2018-08-31Published

2018-04-26Filed