METHOD FOR PRODUCING PLASTICISER FOR PVC DIOCTYL TEREPHTHALATE Russian patent published in 2021 - IPC C07C69/82 C07C67/08 

Abstract RU 2755709 C1

FIELD: polymers.

SUBSTANCE: invention relates to a method for producing plasticisers for polymer materials from processing byproducts, such as terephthaloyl chloride (TCL) waste bottoms. Proposed is a method for producing a plasticiser of dioctyl terephthalate (DOTP) including esterification of terephthaloyl chloride waste bottoms consisting of unreacted terephthalic acid, terephthaloyl chloride and ferric chloride used in the synthesis of TCL as a catalyst, executed in 2 stages, wherein the reaction mass is heated from 91 to 100°C at the first stage, and at the second stage of esterification, the catalyst tetrabutoxytitanium is introduced to execute the synthesis at a temperature of 184 to 200°C.

EFFECT: production of a DOTP plasticiser from terephthaloyl chloride waste bottoms, significantly expanding the raw material source.

1 cl, 3 ex

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RU 2 755 709 C1

Authors

Abdrashitov Yagafar Mukharyamovich

Shapovalov Vitalij Dmitrievich

Fajzullina Nodira Rashidovna

Dates

2021-09-20Published

2020-05-26Filed