FIELD: drilling.
SUBSTANCE: invention relates to a method for producing an invert emulsion emulsifier for drilling fluids, containing an active base in a carbon solvent, by creating the active base by a two-stage condensation reaction of fatty acids of tall pitch with polyalkylene polyamine, for example triethylenetetramine or diethylenetriamine, taken, respectively, in a molar ratio of 1:1-1.1 and 1:2.3 to tall pitch. The condensation reaction is carried out at heating in nitrogen flow with water distillation, at a temperature of 130°C at the first stage, and 180°C – at the second stage. The resulting active base of the emulsifier is dissolved in diesel fuel at a mass ratio, wt.%: active base – 62-60, diesel fuel – 38-40.
EFFECT: providing thermostability of process fluids used in oil production, stability of rheological characteristics and high aggregate stability of drilling fluids, when using the emulsifier.
4 cl, 3 tbl, 3 ex
| Title | Year | Author | Number | 
|---|---|---|---|
| EMULSIFIER FOR INVERT EMULSIONS | 2017 | 
 | RU2697803C2 | 
| IMPROVED INVERT EMULSIFIER FOR USE IN DRILLING MUDS WITH INVERT EMULSION | 2021 | 
 | RU2786172C1 | 
| EMULSIFING AND STABILISING AGENT FOR INVERT EMULSIONS AND METHOD OF PREPARATION OF INVERT EMULSION DRILL MUD ON ITS BASIS | 2007 | 
 | RU2336291C1 | 
| EMULSIFIER FOR INVERT EMULSIONS | 2001 | 
 | RU2200056C2 | 
| INVERT EMULSIONS EMULSIFIER | 2016 | 
 | RU2613975C1 | 
| INVERT EMULSION DRILLING FLUID | 2022 | 
 | RU2783123C1 | 
| EMULSIFIER OF INVERTED EMULSIONS | 2000 | 
 | RU2166988C1 | 
| EMULSIFYING AGENT FOR PREPARATION OF INVERT EMULSIONS | 2001 | 
 | RU2203130C1 | 
| METHOD OF PREPARING ACTIVE BASE INVERT-EMULSION EMULSIFIER, AND INVERSION-EMULSION EMULSIFIER | 2006 | 
 | RU2296614C1 | 
| EMULSIFIER OF INVERT EMULSIONS USED PREDOMINANTLY IN PETROLEUM PRODUCTION | 2004 | 
 | RU2269375C1 | 
Authors
Dates
2021-12-21—Published
2020-12-25—Filed