FIELD: ceramics production.
SUBSTANCE: invention relates to the production of dense structural ceramics from zirconium dioxide. A molding nanopowder with a particle size of zirconium dioxide less than 20 nm, containing (wt.%): calcium oxide 2-5 and baddeleyite concentrate 98-95, is obtained after joint grinding of the components in an aqueous medium for 5 hours using beads from stabilized zirconium dioxide with a diameter of 1.5 mm at a ratio of the mass of the composition of powders of the initial components to the mass of distilled water 1:3, and to the mass of grinding bodies - 1:10 and drying the grinding product at a temperature of 80-90°C for a day at atmospheric pressure. The powder is pressed and sintered at a temperature of 1200-1300°C. In terms of hardness and Young's modulus, zirconium ceramics obtained from the indicated powder containing 2 wt.% CaO corresponds to engineering ceramics from synthetic zirconium dioxide stabilized with yttrium oxide, and surpasses it in terms of crack resistance.
EFFECT: invention allows to produce dense structural ceramics from zirconium dioxide.
1 cl, 4 tbl
| Title | Year | Author | Number | 
|---|---|---|---|
| METHOD OF MAKING CERAMICS BASED ON ZIRCONIUM DIOXIDE | 2018 | 
 | RU2698880C1 | 
| METHOD OF MAKING POROUS ARTICLES OF SPHERICAL SHAPE BASED ON ZIRCONIUM DIOXIDE | 2019 | 
 | RU2731751C1 | 
| METHOD OF PRODUCING ZIRCONIUM CERAMICS | 2019 | 
 | RU2735791C1 | 
| METHOD OF PRODUCING NANOSTRUCTURED COMPOSITE CERAMICS BASED ON ZIRCONIUM, ALUMINUM AND SILICON OXIDES | 2018 | 
 | RU2701765C1 | 
| METHOD FOR PRODUCING HIGH-TEMPERATURE CO SORBENTS | 2020 | 
 | RU2745486C1 | 
| METHOD OF PRODUCTION OF CERAMIC COMPOSITE MATERIAL BASED ON ALUMINIUM AND ZIRCONIUM OXIDES | 2013 | 
 | RU2549945C2 | 
| CERAMIC COMPOSITE MATERIAL | 2018 | 
 | RU2710648C1 | 
| METHOD OF MAKING CERAMIC ARTICLES | 2014 | 
 | RU2545578C1 | 
| METHOD OF PRODUCING DENSE NANOCERAMICS BASED ON ALUMINUM OXIDE IN THE AlO-ZrO(YO) SYSTEM | 2018 | 
 | RU2685604C1 | 
| METHOD OF PRODUCING HOT-PRESSED SILICON CARBIDE CERAMICS | 2023 | 
 | RU2816616C1 | 
Authors
Dates
2022-03-24—Published
2021-08-18—Filed