FIELD: polymer industry.
SUBSTANCE: production of porous polymer films, and in particular a method for obtaining microfiltration membranes used for filtering, analyzing and purifying various media in microbiological, biochemical, pharmaceutical and other industries. A method for producing a cellulose acetate membrane includes the preparation of a molding solution by dissolving cellulose acetates in a mixture of an organic solvent, a precipitant, water and a plasticizer, filtration, thermostatic control, applying a molding solution to a moving metal band, molding and drying. One type of cellulose acetate should be with a low content of associated acetic acid, ranging from 53 to 56 wt.%, and another type of cellulose acetate should be high in bound acetic acid, ranging from 57 to 62 wt.%, polysorbate Twin-80 is added to the molding solution, the molding solution is thermostated for 6 hours at a temperature in the range of 28-30°C, and the molding is carried out at the degree of substitution of the vapor-air mixture of solvents and precipitants with prepared air in the range of 15-20 zone molding volumes per hour.
EFFECT: reduction of the ratio of the maximum pore size to their minimum size to a value not exceeding 1.1-1.2, obtaining a uniform structure with a narrow pore size distribution, reducing the confluent growth of test strain colonies on the membrane surface when microorganisms are isolated from water.
2 cl, 1 dwg, 1 tbl, 1 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCTION OF SEMI-PERMEABLE CELLULOSE ACETATE MEMBRANE | 2005 |
|
RU2296611C2 |
SEMIPERMEABLE ACETATE CELLULOSE MEMBRANE AND A METHOD FOR PREPARATION THEREOF | 2005 |
|
RU2303481C2 |
SEMI-PERMEABLE FLUOROCARBON DIAPHRAGM AND METHOD OF ITS PRODUCING | 2005 |
|
RU2297875C2 |
METHOD OF MANUFACTURING MICROFILTERING MEMBRANES | 1999 |
|
RU2152818C1 |
METHOD OF MODIFYING CELLULOSE ACETATES TO OBTAIN FILTRATION MEMBRANES | 2014 |
|
RU2602151C2 |
MIXTURE FOR FORMATION OF CELLULOSE ACETATE ULTRAFILTRATION MEMBRANE | 2012 |
|
RU2510885C2 |
SUPPORTED POROUS ACETATE-CELLULOSE MEMBRANE AND METHOD OF PREPARATION THEREOF | 2000 |
|
RU2187360C1 |
CELLULOSE ACETATE SEMIPERMEABLE DIAPHRAGM IN THE FORM OF HOLLOW FIBRE, METHOD OF MANUFACTURE OF HOLLOW-FIBRE SEMIPERMEABLE CELLULOSE ACETATE DIAPHRAGM, HEMODIALYZER AND APPARATUS FOR TREATMENT OF EXTRACORPOREAL BLOOD | 1993 |
|
RU2108144C1 |
COMPOSITION FOR PRODUCTION OF SEMI-PERMEABLE POROUS MEMBRANE | 2016 |
|
RU2638981C2 |
MIX FOR FORMING ACETILATION PULP ULTRA FILTRATION MEMBRANE (VERSIONS) | 2010 |
|
RU2426305C1 |
Authors
Dates
2023-05-05—Published
2022-07-04—Filed