FIELD: chemistry of inirganic compounds. SUBSTANCE: elementary phosphorus is subjected to reaction with trimethylamine, ethylene oxide and water at molar ratio of components of 1:(10-20):(8-20) in medium of solvent at temperature of 40-80 C with subsequent treatment of reaction mass with equimolar quantity of sodium hydroxide. Solvent is used in form of isopropanol and water. β-oxyethyltrimethylammonium hydroxide formed in treatment of reaction mass with sodium hydroxide is returned for recycle with elementary phosphorus. EFFECT: reduced toxicity and provided wasteless production method due to recycle of b-pxyethyltrimethylammonium hydroxide in course of reaction. 3 cl
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Authors
Dates
1996-01-20—Published
1989-01-16—Filed