FIELD: chemistry.
SUBSTANCE: invention relates to a method of 1,5-dinitro-3,7-chlordan-1,3,5,7-tetrazene-cyclo-octane production of nitric acid, ammonium nitrate, acetic acid and acetic anhydride, characterised by that, to increase the target product amount, acetate mixture of amino-form, nitric acid and acetic anhydride are added to the ammonium nitrate in acetic acid, and the reaction mixture is held at temperature of 45-50 °C.
EFFECT: technical result is 1,5-dinitro-3,7-chlordan-1,3,5,7-tetrazene-cyclo-octane production with high output.
1 cl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF 1,5-DINITRO-3,7-CHLORDAN-1,3,5,7-TETRAZENE-CYCLO-OCTANE PRODUCTION | 1967 |
|
SU1841152A1 |
| METHOD OF 1,5-DINITRO-3,7-CHLORDAN-1,3,5,7-TETRAZENE-CYCLO-OCTANE PRODUCTION | 1967 |
|
SU1841156A1 |
| METHOD OF SYNTHESIS OF 1,5-DINITRO-3,7-ENDO-METHYLENE-1,3,5,7- TETRAZACYCLOOCTANE | 2001 |
|
RU2198886C1 |
| METHOD OF PRODUCING OCTOGENE | 1969 |
|
SU1841208A1 |
| METHOD OF PRODUCING NONSINTERABLE PULVERULENT AND/OR CRYSTALLINE HEXAMETHYLENE TETRAMINE | 0 |
|
SU1535865A1 |
| METHOD OF PRODUCING 1,3-DIAZIDO-2-NITRO-2-AZAPROPANE | 2010 |
|
RU2440974C1 |
| METHOD OF DIACETATE-2,4,6-TRINITRO-2,4,6-TRIAZAHEPTANEDIOL-1,7 PRODUCING | 1966 |
|
SU1841128A1 |
| METHOD OF PRODUCING OCTOGENE | 1970 |
|
SU1841210A1 |
| METHOD OF SYNTHESIS OF 2,4,6,8,10,12-HEXANITRO-2,4,6,8,10,12-HEXAAZATETRACYCLO-[5,5,0,0, 0]-DODECANE | 2001 |
|
RU2199540C2 |
| METHOD FOR PREPARATION OF WATER-CONTAINING COMMERCIAL GEL-LIKE EXPLOSIVES | 1998 |
|
RU2143661C1 |
