METHOD OF SYNTHESIS OF 2,6-DISUBSTITUTED 2,4,6,8-TETRAAZABICYCLO[3,3,0]OCTANE-3,7-DIONES Russian patent published in 1994 - IPC

Abstract RU 2021273 C1

FIELD: organic chemistry. SUBSTANCE: product of the formula where 1a - R-tert. -butyl, m. p. is 347-349 C or 1b - R - phenyl, m. p. is 375-380 C. Structure is confirmed by data of IR-, NMR- and mass-spectrum. Reagent 1: corresponding mono-N-substituted urea. Reagent 2: glyoxal. Reaction conditions: at 85-90 C in the presence of sulfuric acid in the medium of aqueous isopropanol at the definite ratio of reagents. EFFECT: improved method of synthesis. 2 tbl

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RU 2 021 273 C1

Authors

Jagovkin A.Ju.

Bakibaev A.A.

Filimonov V.D.

Dates

1994-10-15Published

1990-10-15Filed