METHOD FOR PRODUCTION OF 2,4,6,8- TETRACETYL -2,4,6,8- TETRAZABICYCLO[3,3,0]OCTANE- 3,7-DION Russian patent published in 1995 - IPC

Abstract RU 2050358 C1

FIELD: organic chemistry. SUBSTANCE: glycoluril is used as reagent 1, acetic anhydride being used as reagent 2. Reaction is carried out by heating in the presence of perchloric acid till homogenization takes place, the process is followed by adding sodium acetate into reaction mixture and by boiling within 60-65 min. Molar ratio of glycoluril:acetic anhydride: perchloric acid: sodium acetate is 1:(6-8):(0.04-0.08):(0.8-1). Yield of desired product is 89 EFFECT: improves efficiency of method. 1 tbl

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RU 2 050 358 C1

Authors

Jagovkin A.Ju.

Bakibaev A.A.

Filimonov V.D.

Dates

1995-12-20Published

1991-04-29Filed