FIELD: organic chemistry. SUBSTANCE: product: 2-oxo-2-methyl-4-diethylamino-5,5-dimethyl-1,3,2-oxazaphospho- l-3-ine of the formula (I) C9H19N2O2P, empirical formula is C1-C4, yield is 94%. Reagent 1: compound of the formula (II) (C2H5)2NH where R - -alkyl. Reagent 2: . Reaction conditions: ratio of reagents 1 and 2 = 1:(3-5). Process is carried out at the boiling of reaction mixture for 3 h. Synthesized compounds are used in agriculture as plant growth regulating agents. EFFECT: improved method of synthesis.
Title | Year | Author | Number |
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METHOD FOR PREPARING 2-OXO-2-ALKOXY-5,5-DIMETHYL-1,3,2-OXAZAPHOSPHOLIDINE-4-ONES | 2004 |
|
RU2279436C1 |
METHOD FOR PREPARING 2,2-DIMETHYL-4-ALKOXY-5,5-DIMETHYL-1,3,2-OXAZASILOLS | 2003 |
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RU2254339C1 |
METHOD FOR PREPARING 2,2-DIMETHYL-4-ALKOXY-5,5-DIMETHYL-1,3,2-OXAZASILOLS | 2003 |
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RU2254338C1 |
METHOD OF SYNTHESIS OF 2-(FURYL-2)-1,3-OXAZOLIDINES | 1997 |
|
RU2127272C1 |
0 |
|
SU498313A1 | |
PROCESS FOR PREPARING 2-(2-CHLOROALKOXY)-2-OXO-1,4,2-DIOXAPHOSPHEPANES | 0 |
|
SU1033497A1 |
METHOD OF SYNTHESIS OF α-ADAMANTYL-CONTAINING ALIPHATIC AND SATURATED AROMATIC KETONES | 2000 |
|
RU2186760C2 |
PROCESS FOR PRODUCING 2,2-DIMETHOXY-4,4-DIPHENYL-5-SUBSTITUTED-1,3,2-OXAZAPHOSPH-2-ENES | 0 |
|
SU888496A1 |
METHOD OF PREPARING 1-(ADAMANT-1-YL)ETHYLAMINE AND HOMOLOGUES THEREOF | 1998 |
|
RU2152924C1 |
METHOD OF OBTAINING O-ARYL ETHERS 2-THIO- OR 2-OXO-1,3,2-OXOZOPHOSPORINANE | 1981 |
|
SU1019823A1 |
Authors
Dates
1995-01-09—Published
1991-06-13—Filed