FIELD: production of triarylphosphates. SUBSTANCE: product: mixture P(O)(OR)3, where R is aryl. Reagent 1: POCl3. Reagent 2: phenol-xylenol mixture at ratio of (30-40):(70-60) in terms of mass.%, with use of phenol-xylenol mixture in form of 3.5-xylenol of the synthetic and coal kinds in ratio of 2: 1. Reaction conditions: at 170 C with return of nonreacted phenol mixture to zone of reaction in the amount of 6-10 mas.% instead of fresh phenol-xylenol mixture. EFFECT: higher efficiency. 2 cl, 1 tbl
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Authors
Dates
1995-02-09—Published
1991-04-23—Filed