FIELD: organic chemistry. SUBSTANCE: synthesis of 2,2,4-trimethyl-1,3-pentadiol monoisobutyrate is carried out by ester condensation of isobutyric aldehyde in reactor supplied with a mixer that provides value of Re criteria at the level 600-9000. Catalyst - aqueous solution of sodium hydroxide with additions of sodium-alkynesulfate or sodium-sec.-alkynesulfate at concentrations 0.001-0.1 or 0.005-0.05%, respectively, as for sodium hydroxide aqueous solution. EFFECT: improved method of synthesis. 2 cl, 1 tbl
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Authors
Dates
1995-02-20—Published
1992-03-16—Filed