FIELD: chemical technology. SUBSTANCE: precipitation is carried out in electrolyzer with intermembranous space separated from cathode site by anion-exchange membrane, and from anode site - by cation-exchange membrane. Process is carried out by feeding of tantalum-containing solution in cathode space at the rate 4,1-8,2 g/A ·4 Ta2O5, and potassium fluoride solution in intermembranous space at the rate 2.2-4.4 g/A x 2 h KF, and hydrofluoric acid solution in anode space. Precipitation is carried out at 40-60 C. EFFECT: improved method of product preparing. 3 cl, 1 tbl
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Authors
Dates
1995-03-27—Published
1992-04-08—Filed