FIELD: organic chemistry. SUBSTANCE: desired product has melting point 164-165 C. Cyclopentadiene fraction produced by thermal decomposition of dicyclopentadiene having cyclopentene content 80-96 % and boiling point 38-60 C is used as reagent 1, desired product being added into origin suspension. Maleic anhydride is used as reagent 2, its mass ratio to anhydride of endo-norbornene-2,3-dicarboxylic acid is 1:0.1-0.1. Reaction is carried out in atmosphere of carbon dioxide. EFFECT: improves efficiency of the method. 12 cl, 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF SYNTHESIS OF ENDONORBORNENE-2,3-DICARBOXYLIC ACID ANHYDRIDE | 1992 |
|
RU2021267C1 |
METHOD FOR RECLAIMING OF RUBBER | 1992 |
|
RU2061711C1 |
PROCESS: FOR PREPARING ALKYDE RESIN | 1992 |
|
RU2026314C1 |
PROCESS OF PRODUCTION OF FLUID PRODUCTS FROM HEAVY PETROLEUM PRODUCTS | 1992 |
|
RU2024578C1 |
METHOD FOR PRODUCTION OF UNSATURATED POLYESTER RESIN | 1992 |
|
RU2072368C1 |
PROCESS FOR PREPARING LIQUID PRODUCTS FROM HEAVY PETROLEUM PRODUCTS | 1992 |
|
RU2024577C1 |
METHOD FOR JOINT PRODUCTION OF ISOPRENE AND 3-METHYLBUTENE-1 | 1992 |
|
RU2030374C1 |
PROCESS FOR PREPARING BOTH ISOPRENE AND 3-METHYLBUTENE-1 | 1992 |
|
RU2032649C1 |
METHOD FOR SELECTIVE PREPARATION OF EXO,EXO- AND ENDO,ENDO-DI(2-ETHYLHEXYL)NORBORNENE-2,3-DICARBOXYLATES FROM C5 FRACTION OF LIQUID PYROLYSIS PRODUCTS | 2020 |
|
RU2754913C1 |
METHOD OF PRODUCING 1/-L-(-)-NU-AMINO-ALPHA-OXY-BUTYRYL/KANAMYCIN A | 0 |
|
SU1190988A3 |
Authors
Dates
1995-04-10—Published
1992-04-03—Filed