FIELD: organic chemistry. SUBSTANCE: the product is 2-oxy-4- (meth)acryloyloxybenzophenone of the empirical formula: C17H14O4. The melting point is 76 C. The yield is 85%. Reagent 1: 2,4-dioxybenzophenone. Reagent 2: (meth) a ryloyl chloride. Reaction conditions: heating at 40-60 C in the presence of diethylaniline followed by recovery of the desired product from the reaction mixture by precipitation with a C1-C3 alcohol. EFFECT: improved preparation process.
Title | Year | Author | Number |
---|---|---|---|
PROCESS FOR PREPARING BLUE COLOR-FORMING COMPONENTS OF 2- ACYL AMINO-4,6-DICHLORO-5-METHYLPHENOL | 1992 |
|
RU2041870C1 |
LATEXES OF COPOLYMERS OF BUTYLACRYLATE AND DI-N-SUBSTITUTED ACRYLAMIDE | 0 |
|
SU1819274A3 |
METHOD FOR PRODUCTION OF 6-BROM-2-AMINO-4-NITROPHENOL | 1991 |
|
RU2053223C1 |
METHOD FOR PRODUCTION OF 6-BROM-2-AMINO-4-NITROPHENOL | 1991 |
|
RU2053222C1 |
METHOD FOR PRODUCTION OF 1,2-DIBROM-3,5-DINITROBENZENE | 1991 |
|
RU2053220C1 |
METHOD OF SYNTHESIS OF GLUTACONIC ALDEHYDE DIANIL CHLOROHYDRATE | 1989 |
|
SU1779020A1 |
METHOD OF SYNTHESIS OF CARNOSINE | 1990 |
|
RU2030422C1 |
METHOD FOR PRODUCTION OF 6-BROM-2-AMINO-4-NITROPHENOL | 1992 |
|
RU2053224C1 |
METHOD OF SYNTHESIS OF 2-BROMO-4,6-DINITROANILINE | 1991 |
|
RU2030391C1 |
PROCESS FOR PREPARING 4-AND/OR 6-NITRO-2-AMINOPHENOLS | 1992 |
|
RU2068407C1 |
Authors
Dates
1995-05-10—Published
1992-01-21—Filed