METHOD FOR PRODUCTION OF 6-BROM-2-AMINO-4-NITROPHENOL Russian patent published in 1996 - IPC

Abstract RU 2053224 C1

FIELD: organic chemistry. SUBSTANCE: 2,4-dinitrophenol is used as reagent 1, bromine or bromides of alkali metals being used as reagent 2. Reaction is carried out at 60 C in the presence of oxidizing agent. The process is followed by treatment thus obtained reaction mass with sulfite of alkali metal and by reduction 6-brom-2,4-dinitrophenol. Yield of desired product is 69 %, its melting point being 162-163 C. EFFECT: improves efficiency of the method.

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RU 2 053 224 C1

Authors

Andrievskij A.M.

Avidon S.V.

Kobrinskij I.A.

Al'Tman E.Sh.

Nikonov V.V.

Popov B.N.

Ehssert V.K.

Shevtsova I.N.

Dates

1996-01-27Published

1992-06-29Filed