FIELD: heat carrier. SUBSTANCE: liquids were prepared by interaction of magnesium with a mixture of ethyl chloride, tetraethoxysilane, diethyldichlorosilane and methyltrichlorosilane taken at the molar ratio: ethyl chloride 3.0; tetraethoxysilane 0.749-1.01; diethyldichlorosilane 0.067-0.2; methyltrichlorosilane 1.246-0.35 in toluene medium at 50-100 C following by hydrolysis of prepared mixture of ethyl-substituted silanes, toluene distillation off, catalytic rearrangement of hydrolysis products and distilling for fractions. EFFECT: improved method of preparing. 2 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF SYNTHESIS OF MONOMERS CONTAINING FUNCTIONAL GROUPS FOR SYNTHESIS OF POLYETHYLSILOXANE LIQUIDS | 1992 |
|
RU2036926C1 |
METHOD OF SYNTHESIS OF ETHYL-SUBSTITUTED SILANE MIXTURE | 1992 |
|
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PROCESS FOR PREPARING POLYETHYLSILOXANE FLUIDS | 1992 |
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METHOD OF PREPARING OF POLYETHYLSILOXANE LIQUIDS | 1992 |
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METHOD OF OBTAINING FUNCTIONAL GROUPS-CONTAINING ETHYL-SUBSTITUTED SILANES FOR POLYETHYLSILOXANE LIQUIDS | 1983 |
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SU1203867A1 |
METHOD OF PRODUCING POLYETHYLENESILOXANE FLUIDS | 0 |
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SU1657514A1 |
METHOD FOR PRODUCTION OF MONOMERS WHICH CONTAIN FUNCTIONAL GROUPS FOR SYNTHESIS OF POLYETHYLENE SILOXANE LIQUIDS | 1992 |
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RU2061697C1 |
METHOD OF SYNTHESIS OF MONOMERS CONTAINING FUNCTIONAL GROUPS FOR POLYETHYLSILOXANE LIQUIDS SYNTHESIS | 1992 |
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RU2027718C1 |
PROCESS FOR PRODUCING ETHYL-SUBSTITUTED SILANES | 0 |
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SU1002295A1 |
PROCESS FOR PREPARING MONOMERS CONTAINING FUNCTIONAL GROUPS FOR SYNTHESIS OF POLYETHYLSILOXANE LIQUIDS | 1989 |
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SU1621466A1 |
Authors
Dates
1995-05-10—Published
1992-05-20—Filed