METHOD OF PREPARING OF POLYETHYLSILOXANE LIQUIDS Russian patent published in 1995 - IPC

Abstract RU 2034865 C1

FIELD: chemical technology. SUBSTANCE: method involves interaction of magnesium with a mixture of ethyl chloride, tetraethoxysilane and organotrichlorosilane in toluene medium at 50-100 C following by hydrolysis of prepared mixture of ethyl-substituted silanes, toluene distillation off, catalytic rearrangement of hydrolysis products and distillation for fractions. Phenyltrichlorosilane, dichlorophenyltrichlorosilane, γ-trifluoropropyltrichlorosilane or a mixture of these compounds with methyltrichlorosilane were used as a source of organotrichlorosilane. Prepared liquids were used as heat carriers. EFFECT: improved method of liquid preparing. 2 tbl

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RU2034866C1

RU 2 034 865 C1

Authors

Klokov B.A.

Grishutin Ju.P.

Sobolevskij M.V.

Koroleva T.V.

Tivanov V.D.

Markina E.B.

Shejnina S.Z.

Vlasova T.A.

Skorokhodov I.I.

Dates

1995-05-10Published

1992-08-26Filed