FIELD: organic chemistry. SUBSTANCE: product: succinic acid, empirical formula is C4H6O4, m. p. is 185-187 C. Reagent 1: butadiene rubber. Reagent 2: ozone-air or ozone-oxygen mixture. Reaction conditions: in the medium of tetrachloroethane or pentachloroethane in the presence of water and acetic acid at molar ratio (as butadiene fragment), butadiene rubber:ozone:acetic acid = 1:1:(1-12):(0.3-4.0), respectively, following by additional oxidation of prepared product with ozone-air or ozone-oxygen mixture. EFFECT: improved method of synthesis. 3 cl
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Authors
Dates
1995-06-09—Published
1993-03-25—Filed