FIELD: synthetic rubber industry. SUBSTANCE: method involves copolymerization of conjugated dienes with styrene in solvent medium consisting of 25% benzine and 75% cyclohexane in the presence of butyllithium. Copolymers were isolated by method of water degassing involving solvent rectification and its recovering to copolymerization. Vat residues of solvent rectification containing 20.8-23.9% high-boiling component, 68.4-73.3% solvent, 1.7-2.5% styrene and 4.2-5.2% antioxidant were fed to the mixing with copolymerizate before water degassing. EFFECT: improved method of copolymer synthesis. 1 dwg, 3 tbl
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Authors
Dates
1995-07-20—Published
1991-10-17—Filed