FIELD: organic chemistry. SUBSTANCE: desired product having melting point 212-213 C is prepared by yield 72 ClCH2SiCl3 is used as reagent 1, (C2H5O)3N is used as reagent 2, their ratio being 1:21:(1-4). The process is carried out at (-20)-(60) C. EFFECT: improves efficiency of the method.
Authors
Dates
1995-09-10—Published
1992-11-16—Filed