FIELD: organic chemistry. SUBSTANCE: the product: 5-substituted naphthalene-1-(dimethylene) sulfonylamides: X is naphthalinyl-SO2N-CH2-CH2, X is nitro; phthalimido-, benzyloxycarbonylamino, dimethylamino groups. Reagent 1: 5-substituted sulfonyl chloride. Reagent 2: ethyleneimine. Reaction conditions: in the presence of triethyl amine in a lower alcohol. The desired product is isolated by crystallization from the reaction mixture. EFFECT: more efficient preparation process. 6 tbl
Authors
Dates
1995-12-27—Published
1991-06-28—Filed