FIELD: organic chemistry. SUBSTANCE: bromobenzene is treated by mixture which contains brominating agent, nitric acid or nitrate of alkali metal and sulfuric acid. Thus prepared 1,2-dibrom-3,5-dinitrobenzene is hydrolyzed at 60-65 C by aqueous alkali. Said brominating agent is chosen of group which includes bromine, bromide of alkali metal and ammonium bromide. EFFECT: improves efficiency of method.
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Authors
Dates
1996-01-27—Published
1991-11-21—Filed