FIELD: metalloorganic compounds. SUBSTANCE: method involves the reaction of glycerol with butyl-ortho-titanate at their mole ratio = 11:1 followed by distilling off butanol formed and keeping reaction mass under vacuum at 120 C for 2 hr, not above, dissolving in water at pH = 2-2.5 and keeping at heating up to 90-100 C for 2 hr, not above. Product of unknown structure is synthesized, empirical formula is Ti-[-O-CH2-CH(OH)-CH2(OH)]4•8C3H8O3•47H2O. Product has light-yellow color, gel-like, sweet taste and does not contain any impurities. Product is used in medicine. EFFECT: improved method of synthesis. 2 tbl
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Authors
Dates
1996-01-27—Published
1991-09-27—Filed