PROCESS FOR PREPARING CALCRUM ASCORBINATE Russian patent published in 1996 - IPC

Abstract RU 2057128 C1

FIELD: chemical industry. SUBSTANCE: the product: calcium ascorbinate. Reagent 1: 11-30 wt % aqueous ascorbic acid solution. Reagent 2: calcium carbonate or hydroxide. Reaction conditions: on heating at temperature of not higher than 60 C followed by treatment with carbon, separation of the precipitate and concentration of the filtrate to 50-60 wt %, addition of methanol or ethanol under agitation to the resulting concentrate prior to crystallization of calcium ascorbinate, and thee desired product is crystallized on cooling from +5 C to -10 C and is thereafter removed, washed and dried. EFFECT: more efficient preparation process. 4 cl, 1 tbl

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RU 2 057 128 C1

Authors

Kochetkova L.I.

Chumakov S.I.

Ionin V.N.

Rudenko A.A.

Istomina L.I.

Veterkhanov S.R.

Dates

1996-03-27Published

1992-05-06Filed