PROCESS FOR PREPARING TETRAKIS-μ-(METHOXO)-(METHOXO) PENTAKIS(ACETYLACENATO) COPPER (II), REE (III) OF BARIUM Russian patent published in 1996 - IPC

Abstract RU 2063400 C1

FIELD: organometalic chemistry. SUBSTANCE: product: tetrakis-Cu3Ba2Dy C34H63O19,-(methoxo)-(methoxo)pentakis(acetylacetonato) copper (II), dysprosium (III) of barium, empirical formula: Cu(NO)3, decomposition temperature 240 C. Reagent 1: copper nitrate 3HO.. Reagent 2: rare earth element nitrate. Reagent 3: acetyl acetone. Reaction conditions: reagents 1 and 2 are reacted in absolute methanol in the presence of o-formic ester white heating on water bath followed by addition of reagent 3 at pH of about 8 attained by addition of pyridine. EFFECT: more efficient preparation process.

Similar patents RU2063400C1

Title Year Author Number
TETRAMEROUS HETERONUCLEOUS CURBANITE METHOXOCOMPLEXES OF COBALT (II) - NICKEL (II) WITH 2,4-PENTADIONE OR WITH BIDENTATIC PHENOLS 0
  • Matuzenko G.S.
  • Yampolskaya M.A.
  • Gerbeleu N.V.
  • Simonov Yu.A.
  • Dvorkin A.A.
SU1132516A1
METHOD FOR SYNTHESIS OF CUPRATES OF BARIUM AND RARE-EARTH ELEMENTS 2010
  • Garkushin Ivan Kirillovich
  • Boeva Majsara Karimovna
  • Amineva Natal'Ja Anatol'Evna
  • Il'Tuganov Aleksandr Jakovlevich
RU2489356C2
HETEROMETALLIC NEODYMIUM (III) AND IRON (III) MALATE AND A METHOD FOR PREPARATION THEREOF 2003
  • Shabanova I.V.
  • Frolov V.Ju.
  • Panjushkin V.T.
  • Zelenov V.I.
  • Storozhenko T.P.
RU2255082C2
METHOD FOR SYNTHESIS OF CUPRATES OF RARE-EARTH ELEMENTS AND BARIUM 2008
  • Boeva Majsara Karimovna
  • Garkushin Ivan Kirillovich
  • Amineva Natal'Ja Anatol'Evna
  • Bamburov Vitalij Grigor'Evich
  • Sharafutdinov Dinar Damirovich
  • Vasil'Ev Vladimir Vladislavovich
RU2388695C2
METHOD OF PREPARING METHOXOCOMPLEXES OF COPPER/11/ 0
  • Yampolskaya Margarita Anatolevna
  • Matuzenko Galina Savvichna
  • Ablov Anton Vasilevich
SU690018A1
METHOD FOR PRODUCTION OF SUPERCONDUCTING MATERIAL MBaCuO 1996
  • Jugaj K.N.
  • Sychev S.A.
  • Skutin A.A.
  • Seropjan G.M.
  • Murav'Ev A.B.
RU2104939C1
DI(NITRATE) ACETYLACETONATOBIS (1,10-FENANTROLIN) LANTANOID (III) COMPOUND, SUITABLE FOR USE AS LUMINESCENT ADDITIVE TO INK, AND INK FOR HIDDEN MARKING VALUABLE OBJECTS 2007
  • Mirochnik Anatolij Grigor'Evich
  • Karasev Vladimir Egorovich
RU2373211C2
METHOD FOR PRODUCING SELENIDES (Sr,Eu)LnCuSe (Ln = La, Nd, Sm, Gd-Lu, Sc, Y) OF RHOMBIC SYNGONY 2021
  • Rusejkina Anna Valerevna
  • Grigorev Maksim Vladimirovich
  • Solovev Leonid Aleksandrovich
  • Molokeev Maksim Sergeevich
  • Matigorov Aleksej Valerevich
  • Tretyakov Nikolaj Yurevich
  • Ostapchuk Evgenij Anatolevich
  • Elyshev Andrej Vladimirovich
RU2783926C1
METHOD OF PREPARING RARE-EARTH ELEMENT ACETYLACETONATES 2001
  • Frolov V.Ju.
  • Panjushkin V.T.
  • Zelenov V.I.
RU2191190C1
METHOD OF PREPARING DISSIMILAR-LIGAND COMPLEXES OF RARE-EARTH ELEMENTS WITH ACETYLACETONE AND CIS- OR TRANS-BUTEDIOIC ACID 2002
  • Zelenov V.I.
  • Frolov V.Ju.
  • Shabanova I.V.
  • Panjushkin V.T.
RU2237749C2

RU 2 063 400 C1

Authors

Samus' N.M.

Gandzij M.V.

Tsapkov V.I.

Khoroshun I.V.

Sinitsa I.V.

Dates

1996-07-10Published

1991-11-21Filed