FIELD: organic chemistry. SUBSTANCE: desired salts have formula where R is either ammonium group having common formula (where R1,R2 and R3 are the same or different and represent hydrogen atom, lower alkyl or cycloalkyl) or atom of alkali metal. Desired salts are prepared by interaction of base with pure 3-acetoxy-2-cyclobutene-1-on, 1,3-cyclobutanedion or vat residue being prepared during production of diketen and comprising 3-acetoxy-2-cyclobutene-1-on. Amine having common formula where R1,R2 and R3 are as mentioned above or alcoholate or hydroxide of alkali metal is used as said base. EFFECT: improved quality of desired product. 17 cl
Authors
Dates
1997-05-10—Published
1992-01-31—Filed