FIELD: synthesis of dyes and drugs. SUBSTANCE: process for preparing 1-phenyl-3-methyl pyrazolone-5. Reagent 1: phenyl hydrazine. Reagent 2: acetoacetic acid alkyl ester. Reaction conditions: 1st stage 40-60 C, aqueous medium 10-30 min. 2nd stage 60-100 C, anhydrous medium, acetic acid catalyst. EFFECT: more efficient preparation process.
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Authors
Dates
1997-07-10—Published
1993-09-27—Filed