FIELD: analytical methods. SUBSTANCE: solution to be analyzed for trace concentrations of rhodium is treated by 2,2-dipyridyl to achieve its equilibrium concentration 5.10-3-3.10-2 M, than by hydrazine to its equilibrium concentration 0.5-2.5 g-ion/l, after which pH of solution is adjusted to 3.5-5.5, solution is heated, and intensity of emission is finally measured at 77 K. EFFECT: increased accuracy. 4 tbl
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Authors
Dates
1997-09-27—Published
1991-06-28—Filed