METHOD OF PREPARING PALLADIUM CATALYST FOR SYNTHESIS OF 10-(2,3,4- TRIMETHOXY-6-METHYLPHENYL)DECANOIC ACID ETHYL ESTER Russian patent published in 1998 - IPC

Abstract RU 2102136 C1

FIELD: catalysts for organic syntheses. SUBSTANCE: invention relates to activation techniques for crude catalysts used in syntheses of intermediate products for drugs and vitamins. Palladium catalyst on carbon carrier "Sibunite" is activated by ultrasound with intensity 0.1-3 W/sq.cm for 5-60 s using conical head of ultrasonic emitter which is immersed into glass with catalyst contained in sulfuric acid solution in isopropyl alcohol. EFFECT: intensified activation of catalyst. 3 dwg, 1 tbl

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RU 2 102 136 C1

Authors

Sul'Man Mikhail Gennad'Evich

Shkileva Irina Pavlovna

Sul'Man Ehsfir' Mikhajlovna

Dates

1998-01-20Published

1996-04-02Filed